1. Ho na le likristale tse phahameng tsa conductivity ka seleng ea conductivity.
Tharollo: Ka mor'a ho hloekisa sele ea conductivity ka 1: 1 nitric acid, e hlatsoe ka metsi a hloekisitsoeng.
2. Theuent ha e hloekile ka ho lekaneng.
Tharollo: Ho fetola maemo.
3. Kholomo ea chromatographic e monya lintho tse phahameng tsa conductivity.
Tharollo: Washcolumn ka makhetlo-khetlo le ka ho fapanyetsana ka leseli le metsi.
4. Khetho e fosahetseng ea sekala sa ho metha
Ha ho etsoa tlhahlobo ea li-ion tse ntle, kaha sebopeho sa mokokotlo oa eluate se phahame haholo, khetho ea sekala se tlase haholo se tla lebisa ponts'ong ea boleng bo phahameng haholo ba conductivity.Khetha feela sekala sa ho metha hape.
5. Mohatelli ha a sebetse
Tharollo: Hlahloba hore na sehatelli se buletsoe.
6. Mohlala oa mahloriso o phahame haholo.
Tharollo: Hlakola mohlala.
1. Ho na le li-bubble ka har'a pompo.
Tharollo: Valofo ea ho qeta nako e tsamaisanang le clockwise ea valve ea ho tima pompo, li-bubble tse khathatsang.
2. Cheke ea valve ea pompo e silafetse kapa e senyehile.
Tharollo: Fetola valve ea ho hlahloba kapa u e behe ka har'a tharollo ea 1: 1 ea nitric bakeng sa ho hloekisa ka holimo.
3. Sefepi se ka botlolong ea eluent se silafetse kapa se koetsoe.
Tharollo: Kenya sefe sebaka.
4. Ho tlosoa ha metsi ka mokhoa o sa lekaneng.
Tharollo: Fetola motho ea sa tsebeng letho.
Tharollo: Lekola sebaka se thibileng haufi le moo phallo e leng teng ho bona le ho tlosa ho koala.
1. Lera la filthara ea kholomo le koetsoe.
Tharollo: Tlosa kholomo 'me u lokolle ntlha ea ho kena.Tlosa poleiti ea sieve ka hloko, e kenye ka 1: 1 nitric acid 'me ue hlatsoe ka ultrasonic wave ka metsotso e 30, ebe u e hlatsoa ka metsi a deionized' me ue bokelle hape, khutlisetsa morao ho kopanya chromatograph bakeng sa ho hlatsoa.Hlokomela hore chromatograph ha e khone ho hokahana le tsela ea phallo.
2. Valofo ea ente ea litsela tse tšeletseng e koetsoe.
Tharollo: Lekola sebaka se koalang haufi le tsela ea phallo ho fumana le ho rarolla mathata.
3. Sesepa sa ho hlahloba sa pompo se koetsoe.
Tharollo: Fetola valve ea ho hlahloba kapa u e behe ka har'a tharollo ea 1: 1 ea nitric bakeng sa ho hloekisa ka holimo.
4. Tsela ea ho phalla e koetsoe.
Tharollo: fumana ntlha e koalang ho latela mokhoa oa ho felisa butle-butle ebe o fetola.
5. Lebelo le feteletseng.
Tharollo: Fetola pompo ho tekanyo e nepahetseng ea phallo.
6. Khatello e phahameng ka ho fetisisa ea pompo e behiloe tlaase haholo.
Tharollo: Tlas'a phallo ea mosebetsi ea kholomo ea chromatographic, laola khatello e phahameng ka ho fetisisa ea moeli hore e be 5 MPa ka holim'a khatello ea hona joale ea ho sebetsa.
1. Sesebelisoa ha se sebetse nako e telele ka ho lekaneng joalokaha ho reriloe.
Tharollo: Infusion e tsoelang pele ea leseli ho fihlela lisebelisoa li tsitsitse.
2. Ho na le li-bubble ka har'a pompo.
Tharollo: Valofo ea ho qeta nako e tsamaisanang le clockwise ea valve ea ho tima pompo, li-bubble tse khathatsang.
3. Sefahla sa pipe e kenang ea metsi ea pompo e koetsoe, e hlahisa khatello e mpe tlas'a matla a ho hula le ho hlahisa li-bubble.
Tharollo: Ho fetola filthara kapa ho beha filthara ka 1: 1 1M nitric acid e tla hlatsuoa 5min ka bath ea ultrasonic.
4. Ho na le lipululana kholomong.
Tharollo: Sebelisa lisebelisoa tse lokisitsoeng ke metsi a hloekisitsoeng ho hlatsoa kholomo ka lebelo le tlase ho tlosa lipudula.
5. Ho na le li-bubble tseleng ea ho phalla.
Tharollo: Tlosa kholomo le ho ntša li-bubble ka har'a metsi.
6. Ho na le li-bubble ka seleng ea conductivity, e bakang ho feto-fetoha ha kamehla ha motheo.
Tharollo: Flushing conductivity cel, li-bubble tse khathatsang
7. Voltage ha e tsitsa kapa e kena-kenana le static electrostatic.
Tharollo: Kenya voltage stabilizer ebe u sila sesebelisoa.
1. Nako ea ho futhumatsa pele ea sesebelisoa ha e lekane.
Tharollo: Eketsa nako ea ho futhumatsa pele.
2. Phallo leakage.
Tharollo: fumana sebaka sa ho lutla 'me u se lokise, haeba se sa khone ho rarolloa, khutlisetsa lenonyeletso.
3. Voltage ha e tsitsa kapa e kena-kenana le static electrostatic.
Tharollo: Kenya voltage stabilizer ebe u sila sesebelisoa.
1. Ho tsepama ha motho ea sa tsebeng letho ha hoa nepahala.
Tharollo: Khetha ho tsepamisa mohopolo hantle .
2. Sekhahla sa phallo ea eluentis se phahame haholo.
Tharollo: Khetha lebelo le nepahetseng la phallo ea leseli.
3. Ho sebelisa lisampole tse nang le mahloriso a feteletseng
Tharollo: Hlakola mohlala.
4. Kholomo e silafetse .
Tharollo: Hlahisa kapa u emise kholomo.
1. Bophahamo ba ente ea sampuli ha bo fetohe.
Tharollo: Enta sampole ka bophahamo ba modumo makhetlo a fetang 10 a lesakaneng la bongata ho netefatsa ente e felletseng.
2. Motsoako oa sampole e kentsoeng ha oa nepahala.
Tharollo: Khetha motsoako o nepahetseng oa sampole e kentsoeng.
3. The reagent ha e hloekile.
Tharollo: Kenya sebaka sa reagent.
4. Lintho tse tsoang linaheng tse ling li teng metsing a hloekisitsoeng.
Tharollo: Tlosa metsi a hloekisitsoeng.
5. Phallo ea fetoha.
Tharollo: Fumana mabaka a liphetoho tse joalo 'me u li lokisetse boemo ba pele.
6. Tsela ea ho phalla e koetsoe.
Tharollo: fumana sebaka se koetsoeng, lokisa kapa u etse se seng.
1. Reagent ha e hloekile.
Tharollo: Fetola li-reagents.
2. Metsi a hloekisitsoeng a na le litšila.
Tharollo: Nka sebaka sa metsi a hloekisitsoeng.
1. Ho kenngoa ka mokhoa o fosahetseng oa sele ea conductivity.
Tharollo: Kenya botjha selefounu ya conductivity.
2. Seleng ea conductivity ea conductivity e senyehile.
Tharollo: Kenya sebaka sa sele ea conductivity.
3. Pompo ha e na tharollo ea tlhahiso.
Tharollo: Sheba pontšo ea khatello ho netefatsa hore na pompo e sebetsa.
1. Tharollo e tloaelehileng e silafalitsoe, haholo-holo lisampole tse fokolang haholo.
Tharollo: Lokisetsa tharollo hape.
2. Metsi a hloekisitsoeng ha a hloeka.
Tharollo: nka sebaka sa metsi a deionized.
3. Motsoako oa sampuli o phahame haholo kapa o tlase haholo, ho tsoa moeling oa mohala oa sesebelisoa.
Tharollo: Khetha mofuta o nepahetseng oa ho tsepamisa maikutlo.
Tharollo: fetola thapo ea motlakase kapa phepelo ea motlakase e sa fetoheng.
1. Khase e monngoeng ka phaepheng ea tsela e phallang
Tharollo: ha phepelo ea metsi e bulehile, bula valve ea ho ntša metsi ea pompo, qala pompo ea plunger 'me u lule u thothomela filthara ho tlosa khase ka botlalo.
2. Mocheso o phahameng haholo oa ka tlung o lebisang ho se nang metsi a lekaneng a degasation.
Tharollo: Sebelisa sesebediswa sa ho tlosa kgase inthaneteng.
3. Cheke ea valve ea pompo e silafetse kapa e senyehile.
Tharollo: Fetola valve ea ho hlahloba kapa u e behe ka har'a tharollo ea 1: 1 ea nitric bakeng sa ho hloekisa ka holimo.